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Natural fermentation was carried out mainly by lactic acid bacteria (Leuconostoc spp.) and yeast (Zygosaccharomyces spp. and Pichia spp.). We have previously examined the preparation of novel four trisaccharides from the beverage: O-β-D-fructopyranosyl-(2-\u003e6)-O-β-D-glucopyranosyl-(1-\u003e3)-D-glucopyranose, O-β-D-fructopyranosyl-(2-\u003e6)-O-[β-D-glucopyranosyl-(1-\u003e3)]-D-glucopyranose, O-β-D-glucopyranosyl-(1-\u003e1)-O-β-D-fructofuranosyl-(2\u003c-\u003e1)-α-D-glucopyranoside and O-β-D-galactopyranosyl-(1-\u003e1)-O-β-D-fructofuranosyl-(2\u003c-\u003e1)- α-D-glucopyranoside. Results: Three further novel oligosaccharides have been found from this beverage and isolated from the beverage using carbon-Celite column chromatography and preparative high performance liquid chromatography. Structural confirmation of the saccharides was provided by methylation analysis, MALDI-TOF-MS and NMR measurements. Conclusion: The following novel trisaccharides were identified: O-β-D-fructofuranosyl-(2-\u003e1)-O-[β-D-glucopyranosyl-(1-\u003e3)]-β-D-glucopyranoside (named \"3G-β-D-glucopyranosyl β, β-isosucrose\"), O-β-D-glucopyranosyl-(1-\u003e2)-O-[β-D-glucopyranosyl-(1-\u003e4)]-D-glucopyranose (41-β-D-glucopyranosyl sophorose) and O-β-D-fructofuranosyl-(2-\u003e6)-O-β-D-glucopyranosyl-(1-\u003e3)-D-glucopyranose (62-β-D-fructofuranosyl laminaribiose).", "subitem_description_type": "Abstract"}]}, "item_2_publisher_36": {"attribute_name": "出版者", "attribute_value_mlt": [{"subitem_publisher": "BioMed Central Ltd"}]}, "item_2_relation_14": {"attribute_name": "DOI", "attribute_value_mlt": [{"subitem_relation_type": "isIdenticalTo", "subitem_relation_type_id": {"subitem_relation_type_id_text": "10.1186/1752-153X-3-8", "subitem_relation_type_select": "DOI"}}]}, "item_2_rights_16": {"attribute_name": "権利(URI)", "attribute_value_mlt": [{"subitem_rights": "http://creativecommons.org/licenses/by/2.0/ | http://creativecommons.org/licenses/by/2.0/"}]}, "item_2_source_id_10": {"attribute_name": "ISSN", "attribute_value_mlt": [{"subitem_source_identifier": "1752-153X", "subitem_source_identifier_type": "ISSN"}]}, "item_2_version_type_19": {"attribute_name": "著者版フラグ", "attribute_value_mlt": [{"subitem_version_resource": "http://purl.org/coar/version/c_970fb48d4fbd8a85", "subitem_version_type": "VoR"}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "Okada, Hideki"}], "nameIdentifiers": [{"nameIdentifier": "3009", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Fukushi, Eri"}], "nameIdentifiers": [{"nameIdentifier": "3010", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Yamamori, Akira"}], "nameIdentifiers": [{"nameIdentifier": "3011", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Kawazoe, Naoki"}], "nameIdentifiers": [{"nameIdentifier": "3012", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Onodera, Shuichi"}], "nameIdentifiers": [{"nameIdentifier": "3013", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Kawabata, Jun"}], "nameIdentifiers": [{"nameIdentifier": "3014", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Shiomi, Norio"}], "nameIdentifiers": [{"nameIdentifier": "3015", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2017-09-14"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "S-795_Onodera.pdf", "filesize": [{"value": "426.1 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_free", "mimetype": "application/pdf", "size": 426100.0, "url": {"label": "S-795_Onodera.pdf", "url": "https://rakuno.repo.nii.ac.jp/record/1289/files/S-795_Onodera.pdf"}, "version_id": "c55dccc5-be2a-499d-8a0c-eda5b7abc4d9"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "eng"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "journal article", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts"}]}, "item_type_id": "2", "owner": "3", "path": ["19"], "permalink_uri": "http://hdl.handle.net/10659/1756", "pubdate": {"attribute_name": "公開日", "attribute_value": "2011-03-31"}, "publish_date": "2011-03-31", "publish_status": "0", "recid": "1289", "relation": {}, "relation_version_is_last": true, "title": ["Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts"], "weko_shared_id": -1}
Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts
http://hdl.handle.net/10659/1756
http://hdl.handle.net/10659/17561edbba3b-f707-4cd2-80ed-8c2832805c2e
名前 / ファイル | ライセンス | アクション |
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S-795_Onodera.pdf (426.1 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2011-03-31 | |||||
タイトル | ||||||
タイトル | Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Okada, Hideki
× Okada, Hideki× Fukushi, Eri× Yamamori, Akira× Kawazoe, Naoki× Onodera, Shuichi× Kawabata, Jun× Shiomi, Norio |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Background: A fermented beverage of plant extracts was prepared from about fifty kinds of vegetables and fruits. Natural fermentation was carried out mainly by lactic acid bacteria (Leuconostoc spp.) and yeast (Zygosaccharomyces spp. and Pichia spp.). We have previously examined the preparation of novel four trisaccharides from the beverage: O-β-D-fructopyranosyl-(2->6)-O-β-D-glucopyranosyl-(1->3)-D-glucopyranose, O-β-D-fructopyranosyl-(2->6)-O-[β-D-glucopyranosyl-(1->3)]-D-glucopyranose, O-β-D-glucopyranosyl-(1->1)-O-β-D-fructofuranosyl-(2<->1)-α-D-glucopyranoside and O-β-D-galactopyranosyl-(1->1)-O-β-D-fructofuranosyl-(2<->1)- α-D-glucopyranoside. Results: Three further novel oligosaccharides have been found from this beverage and isolated from the beverage using carbon-Celite column chromatography and preparative high performance liquid chromatography. Structural confirmation of the saccharides was provided by methylation analysis, MALDI-TOF-MS and NMR measurements. Conclusion: The following novel trisaccharides were identified: O-β-D-fructofuranosyl-(2->1)-O-[β-D-glucopyranosyl-(1->3)]-β-D-glucopyranoside (named "3G-β-D-glucopyranosyl β, β-isosucrose"), O-β-D-glucopyranosyl-(1->2)-O-[β-D-glucopyranosyl-(1->4)]-D-glucopyranose (41-β-D-glucopyranosyl sophorose) and O-β-D-fructofuranosyl-(2->6)-O-β-D-glucopyranosyl-(1->3)-D-glucopyranose (62-β-D-fructofuranosyl laminaribiose). | |||||
書誌情報 |
Chemistry Central Journal 巻 3, p. 8-1-8-8, 発行日 2009-07 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 1752-153X | |||||
DOI | ||||||
関連タイプ | isIdenticalTo | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.1186/1752-153X-3-8 | |||||
権利(URI) | ||||||
権利情報 | http://creativecommons.org/licenses/by/2.0/ | http://creativecommons.org/licenses/by/2.0/ | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
出版者 | ||||||
出版者 | BioMed Central Ltd | |||||
資源タイプ | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article |